TY - JOUR
T1 - Simultaneous detection of sulfamethoxazole, diclofenac, carbamazepine, and bezafibrate by solid phase extraction and high performance liquid chromatography with diode array detection
AU - Zhou, Zhengwei
AU - Jiang, Jia-Qian
PY - 2014/5
Y1 - 2014/5
N2 - A method of solid phase extraction (SPE) coupled with high performance liquid chromatography and diode array detection (HPLC-DAD) was studied for the simultaneous determination of sulfamethoxazole (SMX), diclofenac (DCF), carbamazepine (CBZ), and bezafi brate (BZF) in test solutions. The target compounds were extracted by SPE from samples, and the resulting elutes were analyzed using a HPLC-DAD system at wavelengths of 270, 280, 290, and 230 nm for SMX, DCF, CBZ, and BZF, respectively. This method shows good recoveries for SMX, DCF, CBZ, and BZF with mean recoveries of 89.7 ± 9.3%, 86.1 ± 7.6%, 95.0 ± 6.5%, and 94.0 ± 5.4%, respectively.
AB - A method of solid phase extraction (SPE) coupled with high performance liquid chromatography and diode array detection (HPLC-DAD) was studied for the simultaneous determination of sulfamethoxazole (SMX), diclofenac (DCF), carbamazepine (CBZ), and bezafi brate (BZF) in test solutions. The target compounds were extracted by SPE from samples, and the resulting elutes were analyzed using a HPLC-DAD system at wavelengths of 270, 280, 290, and 230 nm for SMX, DCF, CBZ, and BZF, respectively. This method shows good recoveries for SMX, DCF, CBZ, and BZF with mean recoveries of 89.7 ± 9.3%, 86.1 ± 7.6%, 95.0 ± 6.5%, and 94.0 ± 5.4%, respectively.
KW - spectroscopy
KW - solid phase extraction
KW - chromatography
U2 - 10.1007/s10812-014-9921-x
DO - 10.1007/s10812-014-9921-x
M3 - Article
SN - 0021-9037
VL - 81
SP - 273
EP - 278
JO - Journal of Applied Spectroscopy
JF - Journal of Applied Spectroscopy
IS - 2
ER -